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Abstract Radiation measurement relies on pulse detection, which can be performed using various configurations of high-speed analog-to-digital converters (ADCs) and field-programmable gate arrays (FPGAs). For optimal power consumption, design simplicity, system flexibility, and the availability of DSP slices, we consider the Radio Frequency System-on-Chip (RFSoC) to be a more suitable option than traditional setups. To this end, we have developed custom RFSoC-based electronics and verified its feasibility. The ADCs on RFSoC exhibit a flat frequency response of 1–125 MHz. The root-mean-square (RMS) noise level is 2.1 ADC without any digital signal processing. The digital signal processing improves the RMS noise level to 0.8 ADC (input equivalent 40 μV_rms). Baseline correction via digital signal processing can effectively prevent photomultiplier overshoot after a large pulse. Crosstalk between all channels is less than -55 dB. The measured data transfer speed can support up to 32 kHz trigger rates (corresponding to 750 Mbps). Overall, our RFSoC-based electronics are highly suitable for pulse detection, and after some modifications, they will be employed in the Kamioka Liquid Scintillator Anti-Neutrino Detector (KamLAND).